Electropolishing of a Nickel-Titanium-Copper Shape Memory Alloy in Methanolic Sulfuric Acid

Stefanie Drensler, Lakshman Neelakantan, Cristoph Somsen, Gunther Eggeler, Achim Walter Hassel (Editor)

Research output: Contribution to journalArticlepeer-review

Abstract

Electropolishing of NiTiCu shape memory alloy was performed in methanolic sulfuric acid as a surface processing method. The current investigation, using a rotating disk electrode, aims at identifying appropriate electropolishing conditions for this alloy based on understanding the underlying mechanism. The influence of temperature, rotation rate, and sulfuric acid concentration (3 or 5 M H2SO4) was quantified. Electropolishing in methanolic 5 M H2SO4 is solely mass-transport-controlled, while a mixed control is found for the methanolic 3 M H2SO4. This behavior is different from that of the binary NiTi alloy. From the electrochemical perspective, a methanolic 5 M H2SO4 solution is more suitable for electropolishing NiTiCu. The activation energy for electrodissolution is 21.5 kJ mol-1.
Original languageEnglish
Pages (from-to)C1-C4
Number of pages4
JournalElectrochemical and Solid-State Letters
Volume12
Issue number2
DOIs
Publication statusPublished - 2009

Fields of science

  • 104005 Electrochemistry
  • 104006 Solid state chemistry
  • 104014 Surface chemistry
  • 104017 Physical chemistry
  • 105113 Crystallography
  • 105116 Mineralogy
  • 503013 Subject didactics of natural sciences
  • 204 Chemical Process Engineering
  • 204001 Inorganic chemical technology
  • 205016 Materials testing
  • 210006 Nanotechnology
  • 211104 Metallurgy

JKU Focus areas

  • Engineering and Natural Sciences (in general)

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